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Potassium carbonate-silica: A highly effective stationary phase for the chromatographic removal of organotin impurities

Harrowven, DC and Curran, DP and Kostiuk, SL and Wallis-Guy, IL and Whiting, S and Stenning, KJ and Tang, B and Packard, E and Nanson, L (2010) Potassium carbonate-silica: A highly effective stationary phase for the chromatographic removal of organotin impurities. Chemical Communications, 46 (34). 6335 - 6337. ISSN 1359-7345

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Abstract

Organotin impurities in product mixtures can be reduced from stoichiometric levels to ∼15 parts per million by column chromatography using 10% w/w anhydrous potassium carbonate-silica as a stationary phase. © 2010 The Royal Society of Chemistry.


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Details

Item Type: Article
Status: Published
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Harrowven, DC
Curran, DPcurran@pitt.eduCURRAN
Kostiuk, SL
Wallis-Guy, IL
Whiting, S
Stenning, KJ
Tang, B
Packard, E
Nanson, L
Date: 14 September 2010
Date Type: Publication
Journal or Publication Title: Chemical Communications
Volume: 46
Number: 34
Page Range: 6335 - 6337
DOI or Unique Handle: 10.1039/c0cc01328e
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Refereed: Yes
ISSN: 1359-7345
MeSH Headings: Carbonates--chemistry; Molecular Structure; Organotin Compounds--chemical synthesis; Organotin Compounds--chemistry; Organotin Compounds--isolation & purification; Potassium--chemistry; Silicon Dioxide--chemistry; Stereoisomerism
PubMed ID: 20680210
Date Deposited: 08 Feb 2013 20:58
Last Modified: 15 Oct 2017 06:55
URI: http://d-scholarship.pitt.edu/id/eprint/17267

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