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Fluorous mixture synthesis of four stereoisomers of the C21-C40 fragment of tetrafibricin

Zhang, K and Curran, DP (2010) Fluorous mixture synthesis of four stereoisomers of the C21-C40 fragment of tetrafibricin. Synlett (4). 667 - 671. ISSN 0936-5214

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Abstract

Four stereoisomers of the C21-C40 fragment are synthesized in a single exercise with the aid of fluorous tagging to encode configurations at C37 and C33. After demixing and detagging, the isomers were found to have substantially identical 1H NMR spectra. However, there were some small but reliable differences in their 13C NMR spectra. © Georg Thieme Verlag Stuttgart.


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Details

Item Type: Article
Status: Published
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Zhang, K
Curran, DPcurran@pitt.eduCURRAN
Date: 13 August 2010
Date Type: Publication
Journal or Publication Title: Synlett
Number: 4
Page Range: 667 - 671
DOI or Unique Handle: 10.1055/s-0029-1219376
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Refereed: Yes
ISSN: 0936-5214
PubMed Central ID: PMC2914344
PubMed ID: 20686632
Date Deposited: 14 Mar 2013 14:11
Last Modified: 22 Jun 2021 12:56
URI: http://d-scholarship.pitt.edu/id/eprint/17697

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