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Purification of fluorous Mitsunobu reactions by liquid-liquid extraction

Curran, DP and Bajpai, R and Sanger, E (2006) Purification of fluorous Mitsunobu reactions by liquid-liquid extraction. Advanced Synthesis and Catalysis, 348 (12-13). 1621 - 1624. ISSN 1615-4150

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Abstract

Solvent tuning and partition coefficient measurements have identified suitable reagent and solvent combinations for the purification of fluorous Mitsunobu reaction products. The crude reaction mixtures are partitioned between 2/1 HFE-7100/FC-72 and DMF/10% water to provide reagent (fluorous) and product (organic) fractions. © 2006 Wiley-VCH Verlag GmbH & Co. KGaA.


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Details

Item Type: Article
Status: Published
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Curran, DPcurran@pitt.eduCURRAN
Bajpai, R
Sanger, E
Date: 1 August 2006
Date Type: Publication
Journal or Publication Title: Advanced Synthesis and Catalysis
Volume: 348
Number: 12-13
Page Range: 1621 - 1624
DOI or Unique Handle: 10.1002/adsc.200606187
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Refereed: Yes
ISSN: 1615-4150
Date Deposited: 28 May 2013 14:51
Last Modified: 02 Feb 2019 15:58
URI: http://d-scholarship.pitt.edu/id/eprint/18742

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