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Solution-phase mixture synthesis with double-separation tagging: Double demixing of a single mixture provides a stereoisomer library of 16 individual murisolins

Wilcox, CS and Gudipati, V and Lu, H and Turkyilmaz, S and Curran, DP (2005) Solution-phase mixture synthesis with double-separation tagging: Double demixing of a single mixture provides a stereoisomer library of 16 individual murisolins. Angewandte Chemie - International Edition, 44 (42). 6938 - 6940. ISSN 1433-7851

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Abstract

(Chemical Equation Presented) Two tags are better than one: Sixteen individual stereoisomers of murisolin (see scheme) are synthesized together and isolated in pure form with the aid of a double-separation tagging procedure. A strategy for solution-phase stereoisomer synthesis based on double-separation tagging and double demixing is implemented with fluoroalkyl and oligoethylene glycol (OEG, (OCH2CH2)nOCH3) tags. © 2005 Wiley-VCH Verlag GmbH & Co. KGaA.


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Details

Item Type: Article
Status: Published
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Wilcox, CSdaylite@pitt.eduDAYLITE
Gudipati, V
Lu, H
Turkyilmaz, S
Curran, DPcurran@pitt.eduCURRAN
Date: 28 October 2005
Date Type: Publication
Journal or Publication Title: Angewandte Chemie - International Edition
Volume: 44
Number: 42
Page Range: 6938 - 6940
DOI or Unique Handle: 10.1002/anie.200501989
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Refereed: Yes
ISSN: 1433-7851
MeSH Headings: Furans--chemical synthesis; Furans--chemistry; Lactones--chemical synthesis; Lactones--chemistry; Molecular Structure; Solutions--chemistry; Stereoisomerism; Time Factors; Vanillic Acid--analogs & derivatives; Vanillic Acid--chemical synthesis; Vanillic Acid--chemistry
PubMed ID: 16206309
Date Deposited: 15 Jul 2013 19:56
Last Modified: 02 Feb 2019 15:59
URI: http://d-scholarship.pitt.edu/id/eprint/19281

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