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β-cyclodextrin columns for separation of fluorous and non-fluorous compounds: How to use β-cyclodextrin columns in fluorous mixture synthesis and racemic synthesis

Mikami, K and Matsuzawa, H and Tekeuchi, S and Nakamura, Y and Curran, DP (2004) β-cyclodextrin columns for separation of fluorous and non-fluorous compounds: How to use β-cyclodextrin columns in fluorous mixture synthesis and racemic synthesis. Synlett (15). 2713 - 2716. ISSN 0936-5214

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Abstract

Guidelines for the use of β-cyclodextrin columns in fluorous and non-fluorous mixture synthesis, and racemic synthesis are suggested. Fluorous compounds can be separated more efficiently with SUMICHIRAL OA-7000 and -7100, while non-fluorous compounds can be separated better with SUMICHIRAL OA-7500. When the ratio of water in the mobile phase is large (>20%), the guard column (GL cart) can improve the separability of the fluorinated mixture.


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Details

Item Type: Article
Status: Published
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Mikami, K
Matsuzawa, H
Tekeuchi, S
Nakamura, Y
Curran, DPcurran@pitt.eduCURRAN
Date: 7 December 2004
Date Type: Publication
Journal or Publication Title: Synlett
Number: 15
Page Range: 2713 - 2716
DOI or Unique Handle: 10.1055/s-2004-835649
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Refereed: Yes
ISSN: 0936-5214
Date Deposited: 09 Oct 2013 15:52
Last Modified: 02 Feb 2019 15:58
URI: http://d-scholarship.pitt.edu/id/eprint/19861

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