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Reverse fluorous solid-phase extraction: A new technique for rapid separation of fluorous compounds

Matsugi, M and Curran, DP (2004) Reverse fluorous solid-phase extraction: A new technique for rapid separation of fluorous compounds. Organic Letters, 6 (16). 2717 - 2720. ISSN 1523-7060

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Abstract

Fluorous-tagged compounds can rapidly be separated from organic (non-tagged) compounds by the new separation technique of reverse fluorous solid-phase extraction (r-fspe). In a reversal of the roles of solid and liquid phases in standard fluorous spe, a mixture is charged to a polar solid phase (standard silica gel) and then eluted with a fluorous solvent or solvent mixture. The organic components of the mixture are retained, while the fluorous components pass.


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Details

Item Type: Article
Status: Published
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Matsugi, M
Curran, DPcurran@pitt.eduCURRAN
Date: 5 August 2004
Date Type: Publication
Journal or Publication Title: Organic Letters
Volume: 6
Number: 16
Page Range: 2717 - 2720
DOI or Unique Handle: 10.1021/ol049040o
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Refereed: Yes
ISSN: 1523-7060
MeSH Headings: Chromatography, Gel--methods; Fluorine Compounds--chemistry; Fluorine Compounds--isolation & purification; Organic Chemicals--isolation & purification; Silica Gel; Silicon Dioxide; Solvents--chemistry
PubMed ID: 15281752
Date Deposited: 17 Oct 2013 15:35
Last Modified: 02 Feb 2019 15:58
URI: http://d-scholarship.pitt.edu/id/eprint/19869

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