Nakamura, H and Usui, T and Kuroda, H and Ryu, I and Matsubara, H and Yasuda, S and Curran, DP
(2003)
Fluorous solvent as a new phase-screen medium between reagents and reactants in the bromination and chlorination of alcohols.
Organic Letters, 5 (8).
1167 - 1169.
ISSN 1523-7060
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Abstract
(Matrix presented) A perfluorohexane layer regulates the rate of reagent transport in the bromination and chlorination of alcohols. A fluorous triphasic U-tube method is effective for lighter reagents; the thionyl chloride layer (yellow) vanishes, and the chlorides are obtained from the right top organic layer in the chlorination of alcohols.
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