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Preparation of a fluorous chiral BINOL derivative and application to an asymmetric protonation reaction

Nakamura, Y and Takeuchi, S and Ohgo, Y and Curran, DP (2000) Preparation of a fluorous chiral BINOL derivative and application to an asymmetric protonation reaction. Tetrahedron, 56 (3). 351 - 356. ISSN 0040-4020

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Abstract

Fluorous Chiral Proton Source (R,S)-FDHPEB resulted in a higher enantioselectivity (95% ee) than that of the original nonfluorous (R,S)-DHPEB (87% ee) in an enantioselective protonation of a samarium enolate. (R,S)- FDHPEB was easily recovered by a simple filtration through a fluorous reverse phase silica gel and was recyclable. (C) 2000 Elsevier Science Ltd.


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Details

Item Type: Article
Status: Published
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Nakamura, Y
Takeuchi, S
Ohgo, Y
Curran, DPcurran@pitt.eduCURRAN
Date: 14 January 2000
Date Type: Publication
Journal or Publication Title: Tetrahedron
Volume: 56
Number: 3
Page Range: 351 - 356
DOI or Unique Handle: 10.1016/s0040-4020(99)01004-2
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Refereed: Yes
ISSN: 0040-4020
Date Deposited: 21 Feb 2014 21:05
Last Modified: 02 Feb 2019 15:58
URI: http://d-scholarship.pitt.edu/id/eprint/20618

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