Synthesis of perfluoroalkyl-substituted aryl bromides and their purification over fluorous reverse phase silica

Kainz, S and Luo, Z and Curran, DP and Leitner, W (1998) Synthesis of perfluoroalkyl-substituted aryl bromides and their purification over fluorous reverse phase silica. Synthesis (10). 1425 - 1427. ISSN 0039-7881

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Abstract

(1H,1H,2H,2H-Perfluoroooctyl)-substituted aryl bromides 3a,b were synthesized via copper catalyzed cross-coupling of the iodide 1 with the corresponding arylmagnesium bromides 2a,b. A new, efficient method for the purification of highly fluorinated compounds by column chromatography on fluorous reverse phase silica is also described.

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Details

Item Type:	Article
Status:	Published
Creators/Authors:	Creators Email Pitt Username ORCID Kainz, S Luo, Z Curran, DP curran@pitt.edu CURRAN Leitner, W
Date:	1 January 1998
Date Type:	Publication
Journal or Publication Title:	Synthesis
Number:	10
Page Range:	1425 - 1427
DOI or Unique Handle:	10.1055/s-1998-2186
Schools and Programs:	Dietrich School of Arts and Sciences > Chemistry
Refereed:	Yes
ISSN:	0039-7881
Date Deposited:	07 Aug 2014 17:01
Last Modified:	19 Jan 2019 14:55
URI:	http://d-scholarship.pitt.edu/id/eprint/22642

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