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An Efficient Preparation of 3-Perfluorooctyl-1-Chloromethoxypropane and Application of the Fluorous MOMCL in Tagging Hydroxyl and Amine Groups

Ogoe, Claude (2006) An Efficient Preparation of 3-Perfluorooctyl-1-Chloromethoxypropane and Application of the Fluorous MOMCL in Tagging Hydroxyl and Amine Groups. Master's Thesis, University of Pittsburgh. (Unpublished)

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Abstract

A fluorous MOMCl has been synthesized and the preparation is amenable to a 10g scale synthesis. Tagging of both primary and secondary alcohols were achieved in good to excellent yield. Successful detagging was achieved in most cases by employing Lewis or Bronsted acid conditions.


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Details

Item Type: University of Pittsburgh ETD
Status: Unpublished
Creators/Authors:
CreatorsEmailPitt UsernameORCID
Ogoe, Claudecao10@pitt.eduCAO10
ETD Committee:
TitleMemberEmail AddressPitt UsernameORCID
Committee ChairCurran, Dennis Pcurran@pitt.eduCURRAN
Committee MemberFloreancig, Paulflorean@pitt.eduFLOREAN
Committee MemberWipf, Peterpwipf@pitt.eduPWIPF
Date: 29 June 2006
Date Type: Completion
Defense Date: 21 April 2006
Approval Date: 29 June 2006
Submission Date: 28 April 2006
Access Restriction: No restriction; Release the ETD for access worldwide immediately.
Institution: University of Pittsburgh
Schools and Programs: Dietrich School of Arts and Sciences > Chemistry
Degree: MS - Master of Science
Thesis Type: Master's Thesis
Refereed: Yes
Uncontrolled Keywords: Fluorous Chemistry
Other ID: http://etd.library.pitt.edu/ETD/available/etd-04282006-102725/, etd-04282006-102725
Date Deposited: 10 Nov 2011 19:42
Last Modified: 15 Nov 2016 13:42
URI: http://d-scholarship.pitt.edu/id/eprint/7707

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