Martucci, Michael Thomas
(2009)
DEVELOPMENT OF PHOTO-SENSITIZED PRECIPITONS AND STUDIES TOWARD THEIR USE AS LIGHT-ACTIVACTED, REVERSIBLE PHASE TAGS.
Master's Thesis, University of Pittsburgh.
(Unpublished)
Abstract
This dissertation chronicles the discovery and development of an intermolecular photosensitized trans to cis isomerization protocol for bi-phenyl phenyl precipiton phase tags. The optimization of reaction and irradiation conditions, scale-up experiments and isomerization kinetics are presented. This class of precipiton can now be used as a dynamic reversible phase tag ideally suited for multi-step synthesis on multi-gram scale
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Details
| Item Type: |
University of Pittsburgh ETD
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| Status: |
Unpublished |
| Creators/Authors: |
|
| ETD Committee: |
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| Date: |
22 January 2009 |
| Date Type: |
Completion |
| Defense Date: |
13 November 2003 |
| Approval Date: |
22 January 2009 |
| Submission Date: |
4 August 2008 |
| Access Restriction: |
5 year -- Restrict access to University of Pittsburgh for a period of 5 years. |
| Institution: |
University of Pittsburgh |
| Schools and Programs: |
Dietrich School of Arts and Sciences > Chemistry |
| Degree: |
MS - Master of Science |
| Thesis Type: |
Master's Thesis |
| Refereed: |
Yes |
| Uncontrolled Keywords: |
organic synthesis; photosensitizer; precipiton; phase tag; separation |
| Other ID: |
http://etd.library.pitt.edu/ETD/available/etd-08042008-115807/, etd-08042008-115807 |
| Date Deposited: |
10 Nov 2011 19:57 |
| Last Modified: |
15 Nov 2016 13:48 |
| URI: |
http://d-scholarship.pitt.edu/id/eprint/8881 |
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